Structures of the CXCR4 chemokine GPCR with small-molecule and cyclic peptide antagonists

Science. 2010 Nov 19;330(6007):1066-71. doi: 10.1126/science.1194396. Epub 2010 Oct 7.

Abstract

Chemokine receptors are critical regulators of cell migration in the context of immune surveillance, inflammation, and development. The G protein-coupled chemokine receptor CXCR4 is specifically implicated in cancer metastasis and HIV-1 infection. Here we report five independent crystal structures of CXCR4 bound to an antagonist small molecule IT1t and a cyclic peptide CVX15 at 2.5 to 3.2 angstrom resolution. All structures reveal a consistent homodimer with an interface including helices V and VI that may be involved in regulating signaling. The location and shape of the ligand-binding sites differ from other G protein-coupled receptors and are closer to the extracellular surface. These structures provide new clues about the interactions between CXCR4 and its natural ligand CXCL12, and with the HIV-1 glycoprotein gp120.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Animals
  • Cell Line
  • Chemokine CXCL12
  • Crystallography, X-Ray
  • HIV Envelope Protein gp120 / metabolism
  • Humans
  • Membrane Proteins
  • Models, Molecular
  • Protein Binding
  • Protein Conformation
  • Protein Multimerization
  • Receptors, CXCR4 / antagonists & inhibitors
  • Receptors, CXCR4 / chemistry*
  • Receptors, CXCR4 / metabolism
  • Recombinant Proteins / chemistry
  • Spodoptera
  • Thiourea / analogs & derivatives
  • Thiourea / chemistry

Substances

  • Chemokine CXCL12
  • HIV Envelope Protein gp120
  • Membrane Proteins
  • RTL8C protein, human
  • Receptors, CXCR4
  • Recombinant Proteins
  • Thiourea

Associated data

  • PDB/3ODU
  • PDB/3OE0
  • PDB/3OE6
  • PDB/3OE8
  • PDB/3OE9