Discovery of potent isoxazoline glycoprotein IIb/IIIa receptor antagonists

J Med Chem. 1997 Jan 3;40(1):50-60. doi: 10.1021/jm960626t.

Abstract

Using the isoxazoline as a common structural feature, three series of glycoprotein IIb/IIIa receptor antagonists were evaluated, culminating in the discovery of XR299 (30). In an in vitro assay of platelet inhibition, XR299 had an IC50 of 0.24 microM and was a potent antiplatelet agent when dosed intravenously in a canine model. It was shown through X-ray studies of the cinchonidine salt 49 that the receptor required the 5(R)-stereochemistry for high potency. The ethyl ester prodrug of XR299, XR300 (29), was orally active in the dog.

MeSH terms

  • Animals
  • Crystallography, X-Ray
  • Dogs
  • Isoxazoles / chemical synthesis*
  • Isoxazoles / chemistry*
  • Isoxazoles / metabolism
  • Platelet Glycoprotein GPIIb-IIIa Complex / antagonists & inhibitors*
  • Protein Conformation

Substances

  • Isoxazoles
  • Platelet Glycoprotein GPIIb-IIIa Complex
  • XR 299