Imaging the Raf-MEK-ERK Signaling Cascade in Living Cells

Int J Mol Sci. 2024 Oct 1;25(19):10587. doi: 10.3390/ijms251910587.

Abstract

Conventional biochemical methods for studying cellular signaling cascades have relied on destructive cell disruption. In contrast, the live cell imaging of fluorescent-tagged transfected proteins offers a non-invasive approach to understanding signal transduction events. One strategy involves monitoring the phosphorylation-dependent shuttling of a fluorescent-labeled kinase between the nucleus and cytoplasm using nuclear localization, export signals, or both. In this paper, we introduce a simple method to visualize intracellular signal transduction in live cells by exploring the translocation properties of PKC from the cytoplasm to the membrane. We fused bait protein to PKC, allowing the bait (RFP-labeled) and target (GFP-labeled) proteins to co-translocate from the cytoplasm to the membrane. However, in non-interacting protein pairs, only the bait protein was translocated to the plasma membrane. To verify our approach, we examined the Raf-MEK-ERK signaling cascade (ERK pathway). We successfully visualized direct Raf1/MEK2 interaction and the KSR1-containing ternary complex (Raf1/MEK2/KSR1). However, the interaction between MEK and ERK was dependent on the presence of the KSR1 scaffold protein under our experimental conditions.

Keywords: ERK pathway; Raf–MEK–ERK signaling cascade; cell-based assay; scaffold protein; visualizing protein interaction.

MeSH terms

  • Animals
  • Cell Membrane / metabolism
  • Cytoplasm / metabolism
  • Green Fluorescent Proteins / genetics
  • Green Fluorescent Proteins / metabolism
  • HeLa Cells
  • Humans
  • MAP Kinase Kinase 2 / metabolism
  • MAP Kinase Signaling System*
  • Phosphorylation
  • Protein Kinase C / metabolism
  • Protein Kinases
  • Protein Transport
  • Proto-Oncogene Proteins c-raf* / metabolism
  • raf Kinases / metabolism

Substances

  • Proto-Oncogene Proteins c-raf
  • KSR-1 protein kinase
  • Raf1 protein, human
  • MAP Kinase Kinase 2
  • raf Kinases
  • Protein Kinase C
  • Green Fluorescent Proteins
  • Protein Kinases