New withanolides from leaves along with alkyl glucoside from roots and stem as well as variations in withanolide contents in leaves of accessions of Withania somnifera, Ashwagandha- the Indian ginseng$

J Asian Nat Prod Res. 2024 Sep;26(9):1009-1023. doi: 10.1080/10286020.2024.2308184. Epub 2024 Feb 4.

Abstract

Based on the major components in the leaves, the ashwagandha has been found to exist in several chemotypic forms in India. From the leaves of various accessions of Withania somnifera, which were maintained in our institute, three new steroids namely, 4-acetoxy-20β-hydroxy-1-oxo-witha-2,5,24-trienolide (7), 24,25-dihydro-14α-hydroxy withanolide D (9), 5α,6β,17α,27-tetrahydroxy-1-oxo-witha-2,24-dienolide (12) together with thirteen known withanolides were identified by spectroscopic methods. From the roots and stem of one accession and leaves of another, a new alkyl ester glucoside (4) has also been isolated. The new withanolides 7, 9 and 12 have been tentatively named as withanolide 135 A, withanolide 135B and withanolide 108, respectively.

Keywords: Ashwagandha; Chemotypes; Solanaceae; Withania somnifera; steroidal lactone; withanolides; withasteroids.

MeSH terms

  • Glucosides* / chemistry
  • India
  • Molecular Structure
  • Panax / chemistry
  • Plant Extracts
  • Plant Leaves* / chemistry
  • Plant Roots* / chemistry
  • Plant Stems* / chemistry
  • Withania* / chemistry
  • Withanolides* / chemistry

Substances

  • Withanolides
  • Glucosides
  • Ashwagandha
  • Plant Extracts