Rebamipide and Derivatives are Potent, Selective Inhibitors of Histidine Phosphatase Activity of the Suppressor of T Cell Receptor Signaling Proteins

J Med Chem. 2024 Feb 8;67(3):1949-1960. doi: 10.1021/acs.jmedchem.3c01763. Epub 2024 Jan 22.

Abstract

The suppressor of T cell receptor signaling (Sts) proteins are negative regulators of immune signaling. Genetic inactivation of these proteins leads to significant resistance to infection. From a 590,000 compound high-throughput screen, we identified the 2-(1H)-quinolinone derivative, rebamipide, as a putative inhibitor of Sts phosphatase activity. Rebamipide, and a small library of derivatives, are competitive, selective inhibitors of Sts-1 with IC50 values from low to submicromolar. SAR analysis indicates that the quinolinone, the acid, and the amide moieties are all essential for activity. A crystal structure confirmed the SAR and reveals key interactions between this class of compound and the protein. Although rebamipide has poor cell permeability, we demonstrated that a liposomal preparation can inactivate the phosphatase activity of Sts-1 in cells. These studies demonstrate that Sts-1 enzyme activity can be pharmacologically inactivated and provide foundational tools and insights for the development of immune-enhancing therapies that target the Sts proteins.

MeSH terms

  • Alanine / analogs & derivatives*
  • Enzyme Inhibitors
  • Histidine*
  • Phosphoric Monoester Hydrolases / chemistry
  • Quinolones* / pharmacology
  • Receptors, Antigen, T-Cell

Substances

  • rebamipide
  • Histidine
  • Receptors, Antigen, T-Cell
  • Quinolones
  • Phosphoric Monoester Hydrolases
  • Enzyme Inhibitors
  • Alanine