cis-Decalin-containing tetramic acids as inhibitors of insect steroidogenic glutathione S-transferase Noppera-bo

PLoS One. 2023 Aug 31;18(8):e0290851. doi: 10.1371/journal.pone.0290851. eCollection 2023.

Abstract

Decalin-containing tetramic acid is a bioactive scaffold primarily produced by filamentous fungi. The structural diversity of this group of compounds is generated by characteristic enzymes of fungal biosynthetic pathways, including polyketide synthase/nonribosomal peptide synthetase hybrid enzymes and decalin synthase, which are responsible for the construction of a linear polyenoyl tetramic acid structure and stereoselective decalin formation via the intramolecular Diels-Alder reaction, respectively. Compounds that differed only in the decalin configuration were collected from genetically engineered mutants derived from decalin-containing tetramic acid-producing fungi and used for a structure-activity relationship study. Our evaluation of biological activities, such as cytotoxicity against several cancer cell lines and antibacterial, antifungal, antimalarial, and mitochondrial inhibitory activities, demonstrated that the activity for each assay varies depending on the decalin configurations. In addition to these known biological activities, we revealed that the compounds showed inhibitory activity against the insect steroidogenic glutathione S-transferase Noppera-bo. Engineering the decalin configurations would be useful not only to find derivatives with better biological activities but also to discover overlooked biological activities.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anti-Bacterial Agents*
  • Glutathione Transferase* / genetics
  • Insecta

Substances

  • Glutathione Transferase
  • decalin
  • tetramic acid
  • Anti-Bacterial Agents

Grants and funding

This work was supported by JSPS KAKENHI (Grant numbers 18K19163 to RN, 19H04665 and 20K05872 to NK, and 21H04718 to RN, NK, and KM) and the Support for Pioneering Research Initiated by the Next Generation, Japan Science and Technology Agency (JST SPRING; Grant number JPMJSP2124). KE received a fellowship from JST SPRING. The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.