Redesign of Rifamycin Antibiotics to Overcome ADP-Ribosylation-Mediated Resistance

Angew Chem Int Ed Engl. 2022 Nov 7;61(45):e202211498. doi: 10.1002/anie.202211498. Epub 2022 Oct 12.

Abstract

Rifamycin antibiotics are a valuable class of antimicrobials for treating infections by mycobacteria and other persistent bacteria owing to their potent bactericidal activity against replicating and non-replicating pathogens. However, the clinical utility of rifamycins against Mycobacterium abscessus is seriously compromised by a novel resistance mechanism, namely, rifamycin inactivation by ADP-ribosylation. Using a structure-based approach, we rationally redesign rifamycins through strategic modification of the ansa-chain to block ADP-ribosylation while preserving on-target activity. Validated by a combination of biochemical, structural, and microbiological studies, the most potent analogs overcome ADP-ribosylation, restored their intrinsic low nanomolar activity and demonstrated significant in vivo antibacterial efficacy. Further optimization by tuning drug disposition properties afforded a preclinical candidate with remarkable potency and an outstanding pharmacokinetic profile.

Keywords: Antibiotic Resistance; Antibiotics; Drug Design; Mycobacterium Abscessus; Rifamycin.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • ADP-Ribosylation
  • Anti-Bacterial Agents / chemistry
  • Anti-Bacterial Agents / pharmacology
  • Microbial Sensitivity Tests
  • Mycobacterium*
  • Rifamycins* / chemistry
  • Rifamycins* / pharmacology

Substances

  • Anti-Bacterial Agents
  • Rifamycins