Heat treatment dependent cytotoxicity of silicalite-1 films deposited on Ti-6Al-4V alloy evaluated by bone-derived cells

Sci Rep. 2020 Jun 11;10(1):9456. doi: 10.1038/s41598-020-66228-x.

Abstract

A silicalite-1 film (SF) deposited on Ti-6Al-4V alloy was investigated in this study as a promising coating for metallic implants. Two forms of SFs were prepared: as-synthesized SFs (SF-RT), and SFs heated up to 500 °C (SF-500) to remove the excess of template species from the SF surface. The SFs were characterized in detail by X-ray photoelectron spectroscopy (XPS), by Fourier transform infrared spectroscopy (FTIR), by scanning electron microscopy (SEM) and water contact angle measurements (WCA). Two types of bone-derived cells (hFOB 1.19 non-tumor fetal osteoblast cell line and U-2 OS osteosarcoma cell line) were used for a biocompatibility assessment. The initial adhesion of hFOB 1.19 cells, evaluated by cell numbers and cell spreading area, was better supported by SF-500 than by SF-RT. While no increase in cell membrane damage, in ROS generation and in TNF-alpha secretion of bone-derived cells grown on both SFs was found, gamma H2AX staining revealed an elevated DNA damage response of U-2 OS cells grown on heat-treated samples (SF-500). This study also discusses differences between osteosarcoma cell lines and non-tumor osteoblastic cells, stressing the importance of choosing the right cell type model.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alloys
  • Biocompatible Materials / chemistry
  • Cell Line
  • Cell Line, Tumor
  • Cell Membrane / drug effects
  • Cell Proliferation / drug effects
  • Cytotoxins / chemistry
  • Cytotoxins / pharmacology*
  • Hot Temperature
  • Humans
  • Materials Testing / methods
  • Microscopy, Electron, Scanning / methods
  • Osteoblasts / drug effects*
  • Osteocytes / drug effects*
  • Photoelectron Spectroscopy / methods
  • Surface Properties / drug effects
  • Titanium / chemistry*

Substances

  • Alloys
  • Biocompatible Materials
  • Cytotoxins
  • titanium alloy (TiAl6V4)
  • Titanium