In silico, in vitro and in vivo evaluation of natural Bignoniaceous naphthoquinones in comparison with atovaquone targeting the selection of potential antimalarial candidates

Toxicol Appl Pharmacol. 2020 Aug 15:401:115074. doi: 10.1016/j.taap.2020.115074. Epub 2020 May 26.

Abstract

The natural naphthoquinones lapachol, α- and β-lapachone are found in Bignoniaceous Brazilian plant species of the Tabebuia genus (synonym Handroanthus) and are recognized for diverse bioactivities, including as antimalarial. The aim of the present work was to perform in silico, in vitro and in vivo studies to evaluating the antimalarial potential of these three naphthoquinones in comparison with atovaquone, a synthetic antimalarial. The ADMET properties of these compounds were predicted in silico by the preADMET program. The in vitro toxicity assays were experimentally determined in immortalized and tumoral cells from different organs. In vivo acute oral toxicity was also evaluated for lapachol. Several favorable pharmacokinetics data were predicted although, as expected, high cytotoxicity was experimentally determined for β-lapachone. Lapachol was not cytotoxic or showed low cytotoxicity to all of the cells assayed (HepG2, A549, Neuro 2A, LLC-PK1, MRC-5), it was nontoxic in the acute oral test and disclosed the best parasite selectivity index in the in vitro assays against chloroquine resistant Plasmodium falciparum W2 strain. On the other hand, α- and β-lapachone were more potent than lapachol in the antiplasmodial assays but with low parasite selectivity due to their cytotoxicity. The diversity of data here reported disclosed lapachol as a promising candidate to antimalarial drug development.

Keywords: ADMET; Acute oral toxicity; Atovaquone; In silico and in vitro toxicology; Lapachol; Malaria; α- and β-lapachone.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • A549 Cells
  • Animals
  • Antimalarials / administration & dosage*
  • Atovaquone / administration & dosage*
  • Caco-2 Cells
  • Computer Simulation*
  • Dogs
  • Drug Delivery Systems / methods*
  • Drug Evaluation, Preclinical / methods
  • Female
  • Hep G2 Cells
  • Humans
  • LLC-PK1 Cells
  • Madin Darby Canine Kidney Cells
  • Mice
  • Naphthoquinones / administration & dosage*
  • Naphthoquinones / isolation & purification
  • Plasmodium falciparum / drug effects*
  • Plasmodium falciparum / physiology
  • Swine

Substances

  • Antimalarials
  • Naphthoquinones
  • lapachol
  • Atovaquone