Preparation of Composite Filters Based on Porous Coordination Polymers by Using a Vacuum Filtration Method for Highly Efficient Removal of Particulate Matters

Chem Asian J. 2019 Jul 1;14(13):2291-2301. doi: 10.1002/asia.201900464. Epub 2019 May 28.

Abstract

In this study, two novel crystal materials pcp1 and pcp1-L have been synthesized successfully. The different conformations of the two crystals are mainly attributed to the introduction of the Schiff-base ligand L (L=(E)-4-methyl-N-((6-methoxypyridin-2-yl)methylene)aniline). Subsequently, pcp1 and pcp1-L composites have been firstly produced by a vacuum filtration method on various substrates (i.e., melamine foam, plastic mesh, carbon fiber cloth and glass cloth). The obtained robust composites show excellent performance in removing PMs owing to high ζ potential, microporous structure, large conjugation system and electron cloud-exposed metal center (DFT calculations) of pcp1 and pcp1-L. Particularly, pcp1-L@glass cloth with low pressure drop exhibits high thermal stability and high long-term reproducibility. Additionally, the high removal efficiency of pcp1-L@glass cloth towards particulate matters could also be maintained, even achieving >99.9 % in the car exhaust gas field test.

Keywords: composite filter materials; density functoinal calculations; porous coordination polymers; removal of particulate matters; vacuum filtration.