Single-molecule peptide fingerprinting

Proc Natl Acad Sci U S A. 2018 Mar 27;115(13):3338-3343. doi: 10.1073/pnas.1707207115. Epub 2018 Mar 12.

Abstract

Proteomic analyses provide essential information on molecular pathways of cellular systems and the state of a living organism. Mass spectrometry is currently the first choice for proteomic analysis. However, the requirement for a large amount of sample renders a small-scale proteomics study challenging. Here, we demonstrate a proof of concept of single-molecule FRET-based protein fingerprinting. We harnessed the AAA+ protease ClpXP to scan peptides. By using donor fluorophore-labeled ClpP, we sequentially read out FRET signals from acceptor-labeled amino acids of peptides. The repurposed ClpXP exhibits unidirectional processing with high processivity and has the potential to detect low-abundance proteins. Our technique is a promising approach for sequencing protein substrates using a small amount of sample.

Keywords: ClpXP; peptides; protein analysis; single-molecule FRET; single-molecule protein sequencing.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Endopeptidase Clp / chemistry
  • Endopeptidase Clp / metabolism*
  • Escherichia coli Proteins / chemistry
  • Escherichia coli Proteins / metabolism*
  • Fluorescence
  • Fluorescent Dyes / chemistry*
  • Humans
  • Microscopy, Fluorescence / methods*
  • Peptide Fragments / analysis*
  • Peptide Mapping / methods*
  • Proteomics / methods*

Substances

  • Escherichia coli Proteins
  • Fluorescent Dyes
  • Peptide Fragments
  • ClpXP protease, E coli
  • Endopeptidase Clp