International standards for monoclonal antibodies to support pre- and post-marketing product consistency: Evaluation of a candidate international standard for the bioactivities of rituximab

MAbs. 2018 Jan;10(1):129-142. doi: 10.1080/19420862.2017.1386824. Epub 2017 Nov 3.

Abstract

The intrinsic complexity and heterogeneity of therapeutic monoclonal antibodies is built into the biosimilarity paradigm where critical quality attributes are controlled in exhaustive comparability studies with the reference medicinal product. The long-term success of biosimilars will depend on reassuring healthcare professionals and patients of consistent product quality, safety and efficacy. With this aim, the World Health Organization has endorsed the need for public bioactivity standards for therapeutic monoclonal antibodies in support of current controls. We have developed a candidate international potency standard for rituximab that was evaluated in a multi-center collaborative study using participants' own qualified Fc-effector function and cell-based binding bioassays. Dose-response curve model parameters were shown to reflect similar behavior amongst rituximab preparations, albeit with some differences in potency. In the absence of a common reference standard, potency estimates were in poor agreement amongst laboratories, but the use of the candidate preparation significantly reduced this variability. Our results suggest that the candidate rituximab standard can support bioassay performance and improve data harmonization, which when implemented will promote consistency of rituximab products over their life-cycles. This data provides the first scientific evidence that a classical standardization exercise allowing traceability of bioassay data to an international standard is also applicable to rituximab. However, we submit that this new type of international standard needs to be used appropriately and its role not to be mistaken with that of the reference medicinal product.

Keywords: ADCC; CDC; Fc-effector functions; bioactivity; bioassay; biosimilars; international standard; monoclonal antibodies; rituximab.

Publication types

  • Comparative Study
  • Evaluation Study
  • Multicenter Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biological Assay / methods
  • Biological Assay / standards*
  • Biosimilar Pharmaceuticals / pharmacology
  • Biosimilar Pharmaceuticals / standards*
  • Calibration
  • Dose-Response Relationship, Drug
  • Drug Development / methods
  • Drug Development / standards*
  • Drug Stability
  • Immunologic Factors / pharmacology
  • Immunologic Factors / standards*
  • Observer Variation
  • Product Surveillance, Postmarketing / methods
  • Product Surveillance, Postmarketing / standards*
  • Proteolysis
  • Quality Control*
  • Reference Standards
  • Reproducibility of Results
  • Rituximab* / pharmacology
  • Technology, Pharmaceutical / methods
  • Technology, Pharmaceutical / standards*

Substances

  • Biosimilar Pharmaceuticals
  • Immunologic Factors
  • Rituximab