Design, synthesis, and structure-activity relationship studies of novel pleuromutilin derivatives having a piperazine ring

Chem Biol Drug Des. 2016 Nov;88(5):699-709. doi: 10.1111/cbdd.12799. Epub 2016 Jul 9.

Abstract

A series of novel pleuromutilin derivatives possessing piperazine moieties were synthesized under mild conditions. The in vitro antibacterial activities of these derivatives against Staphylococcus aureus and Escherichia coli were tested by the agar dilution method. Structure-activity relationship studies resulted in compounds 11b, 13b, and 14a with the most potent in vitro antibacterial activity among the series (minimal inhibitory concentration = 0.0625-0.125 μg/mL). The binding of compounds 11b, 13b, and 14a to the E. coli ribosome was investigated by molecular modeling, and it was found that there is a reasonable correlation between the binding free energy and the antibacterial activity.

Keywords: drug design; molecular modeling; natural product; structure-based drug design.

MeSH terms

  • Anti-Bacterial Agents / chemical synthesis*
  • Anti-Bacterial Agents / chemistry
  • Anti-Bacterial Agents / pharmacology
  • Binding Sites
  • Diterpenes / chemical synthesis
  • Diterpenes / chemistry
  • Diterpenes / pharmacology
  • Drug Design*
  • Escherichia coli / drug effects
  • Escherichia coli / metabolism
  • Microbial Sensitivity Tests
  • Molecular Docking Simulation
  • Piperazine
  • Piperazines / chemistry*
  • Pleuromutilins
  • Polycyclic Compounds
  • Ribosomes / chemistry
  • Ribosomes / metabolism
  • Staphylococcus aureus / drug effects
  • Structure-Activity Relationship

Substances

  • Anti-Bacterial Agents
  • Diterpenes
  • Piperazines
  • Polycyclic Compounds
  • Piperazine