Glycosylation inhibition reduces cholesterol accumulation in NPC1 protein-deficient cells

Proc Natl Acad Sci U S A. 2015 Dec 1;112(48):14876-81. doi: 10.1073/pnas.1520490112. Epub 2015 Nov 17.

Abstract

Lysosomes are lined with a glycocalyx that protects the limiting membrane from the action of degradative enzymes. We tested the hypothesis that Niemann-Pick type C 1 (NPC1) protein aids the transfer of low density lipoprotein-derived cholesterol across this glycocalyx. A prediction of this model is that cells will be less dependent upon NPC1 if their glycocalyx is decreased in density. Lysosome cholesterol content was significantly lower after treatment of NPC1-deficient human fibroblasts with benzyl-2-acetamido-2-deoxy-α-D-galactopyranoside, an inhibitor of O-linked glycosylation. Direct biochemical measurement of cholesterol showed that lysosomes purified from NPC1-deficient fibroblasts contained at least 30% less cholesterol when O-linked glycosylation was blocked. As an independent means to modify protein glycosylation, we used Chinese hamster ovary ldl-D cells defective in UDP-Gal/UDP-GalNAc 4-epimerase in which N- and O-linked glycosylation can be controlled. CRISPR generated, NPC1-deficient ldl-D cells supplemented with galactose accumulated more cholesterol than those in which sugar addition was blocked. In the absence of galactose supplementation, NPC1-deficient ldl-D cells also transported more cholesterol from lysosomes to the endoplasmic reticulum, as monitored by an increase in cholesteryl [(14)C]-oleate levels. These experiments support a model in which NPC1 protein functions to transfer cholesterol past a lysosomal glycocalyx.

Keywords: cholesterol; glycocalyx; lysosomal glycoprotein; lysosomal storage disease.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Biological Transport, Active / drug effects
  • Biological Transport, Active / genetics
  • CHO Cells
  • Carbohydrate Epimerases / genetics
  • Carbohydrate Epimerases / metabolism
  • Carrier Proteins
  • Cholesterol / genetics
  • Cholesterol / metabolism*
  • Cricetinae
  • Cricetulus
  • Fibroblasts / cytology
  • Fibroblasts / metabolism*
  • Galactose / analogs & derivatives
  • Galactose / pharmacology
  • Glycocalyx / genetics
  • Glycocalyx / metabolism*
  • Glycosylation / drug effects
  • HeLa Cells
  • Humans
  • Intracellular Signaling Peptides and Proteins
  • Lysosomes / genetics
  • Lysosomes / metabolism*
  • Membrane Glycoproteins / deficiency*
  • Niemann-Pick C1 Protein

Substances

  • 1-benzyl-2-acetamido-2-galactopyranoside
  • Carrier Proteins
  • Intracellular Signaling Peptides and Proteins
  • Membrane Glycoproteins
  • NPC1 protein, human
  • Niemann-Pick C1 Protein
  • Cholesterol
  • Carbohydrate Epimerases
  • Galactose