Post-synthesis DNA modifications using a trans-cyclooctene click handle

Org Biomol Chem. 2015 Jan 21;13(3):909-15. doi: 10.1039/c4ob02031f.

Abstract

Post-synthesis DNA modification is a very useful method for DNA functionalization. This is achieved by using a modified NTP, which has a handle for further modifications, replacing the corresponding natural NTP in polymerase-catalyzed DNA synthesis. Subsequently, the handle can be used for further functionalization after PCR, preferably through a very fast reaction. Herein we describe polymerase-mediated incorporation of trans-cyclooctene modified thymidine triphosphate (TCO-TTP). Subsequently, the trans-cyclooctene group was reacted with a tetrazine tethered to other functional groups through a very fast click reaction. The utility of this DNA functionalization method was demonstrated with the incorporation of a boronic acid group and a fluorophore. The same approach was also successfully used in modifying a known aptamer for fluorescent labelling applications.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aptamers, Nucleotide / chemistry
  • Boronic Acids / chemistry
  • Click Chemistry
  • Cyclooctanes / chemistry*
  • DNA / chemistry*
  • DNA Polymerase I / chemistry
  • DNA Primers / chemistry
  • DNA Replication*
  • Fluorescein-5-isothiocyanate
  • Fluorescent Dyes
  • HeLa Cells
  • Heterocyclic Compounds, 1-Ring / chemistry
  • Humans
  • Microscopy, Fluorescence
  • Polymerase Chain Reaction / methods
  • Thymine Nucleotides / chemistry*

Substances

  • Aptamers, Nucleotide
  • Boronic Acids
  • Cyclooctanes
  • DNA Primers
  • Fluorescent Dyes
  • Heterocyclic Compounds, 1-Ring
  • Thymine Nucleotides
  • tetrazine dye 10
  • DNA
  • DNA Polymerase I
  • Fluorescein-5-isothiocyanate
  • thymidine 5'-triphosphate