[Effect of PI3Kδ inhibitor CAL-101 on myeloma cell lines and preliminary study of synergistic effects with other new drugs]

Zhonghua Xue Ye Xue Za Zhi. 2014 Oct;35(10):926-30. doi: 10.3760/cma.j.issn.0253-2727.2014.10.012.
[Article in Chinese]

Abstract

Objective: To investigate the proliferation inhibitory role and mechanism of PI3Kδ inhibitor CAL-101 on multiple myeloma (MM) cells, and to provide new therapeutic options for MM treatment.

Methods: MM cell lines U266 and RPMI8226 cells were treated with various concentrations of CAL-101. MTT assay and CalcuSyn software were performed to determine the inhibitory effect of CAL-101 and the synergistic effect with PCI- 32765, SAHA (suberoylanilide hydroxamic acid), BTZ (Bortezomib) on MM cells. The protein expression level of p-AKT, p-ERK, AKT, ERK and PI3Kδ processed by CAL-101 were analyzed by Western blot.

Results: CAL-101 at concentration of 15, 20, 25, 30 and 40 μmol/L could induce significant dose-dependent proliferation inhibition on U266 cells after treatment for 48 hours. The cell proliferation inhibition rates were (33.54 ± 1.23)%, (41.72 ± 1.78)%, (53.67 ± 2.01)%, (68.97 ± 2.11)% and (79.25 ± 1.92)%, respectively. Similar results were found in RPMI8226 cell line. Western blots showed high expression level of p-AKT, p-ERK, AKT, ERK and PI3Kδ in cell lines and MM primary cells. p-AKT and p-ERK protein expression levels were down-regulated significantly by CAL-101 treatment. Synergistic effect has been verified between CAL-101 and PCI-32765, SAHA and Bortezomib in U266 cell line, and PCI-32765, Bortezomib in RPMI8226 cell line with CI values less than 1.

Conclusion: CAL-101 could inhibit proliferation of MM cell lines. High levels of p-AKT, p-ERK, AKT, ERK and PI3Kδ protein expression were observed in both cell lines and primary cells. Down-regulation of p-AKT and p-ERK probably related with the mechanism of CAL-101 in MM cell proliferation inhibition. CAL-101 has significant synergistic effect with PCI-32765, SAHA and BTZ.

MeSH terms

  • Adenine / analogs & derivatives
  • Boronic Acids
  • Bortezomib
  • Cell Line, Tumor
  • Cell Proliferation
  • Down-Regulation
  • Humans
  • Multiple Myeloma / pathology*
  • Phosphoinositide-3 Kinase Inhibitors*
  • Piperidines
  • Protein Kinase Inhibitors / pharmacology*
  • Purines / pharmacology*
  • Pyrazines
  • Pyrazoles
  • Pyrimidines
  • Quinazolinones / pharmacology*

Substances

  • Boronic Acids
  • Phosphoinositide-3 Kinase Inhibitors
  • Piperidines
  • Protein Kinase Inhibitors
  • Purines
  • Pyrazines
  • Pyrazoles
  • Pyrimidines
  • Quinazolinones
  • ibrutinib
  • Bortezomib
  • Adenine
  • idelalisib