In vivo relaxation behavior of liver compounds at 7 Tesla, measured by single-voxel proton MR spectroscopy

J Magn Reson Imaging. 2014 Dec;40(6):1365-74. doi: 10.1002/jmri.24489. Epub 2013 Nov 12.

Abstract

Purpose: To assess the proton T1 and T2 relaxation of in vivo hepatic water, choline and lipid resonances with possible J-coupling behavior of lipids in healthy volunteers at 7 Tesla (T).

Materials and methods: Relaxation measurements were conducted on corn oil phantoms and on the hepatic tissue of 11 healthy volunteers at 7 T using a surface coil and a STEAM sequence. T1 's were determined by monoexponential fitting, and T2 's by both monoexponential and enhanced-exponential fitting (empirically designed to consider J-coupling of lipid resonances).

Results: In vivo T1 's at 7 T were estimated as follows: water (4.70 ppm), 1362 ± 83 ms; methyl- (0.90 ppm), 1026 ± 162 ms; methylene- (1.30 ppm), 514 ± 25 ms; α-olefinic- (2.02 ppm), 488 ± 220 ms; α-carboxyl- (2.24 ppm), 476 ± 89 ms; diacyl- (2.77 ppm), 479 ± 260 ms group of lipid chains; and choline compounds (3.22 ppm), 1084 ± 52 ms. The T2 's calculated with enhanced fitting were as follows: water, 15 ± 2 ms; methyl-, 34 ± 10 ms; methylene-, 41 ± 8 ms; α-olefinic-, 44 ± 19 ms; α-carboxyl-, 39 ± 15 ms; diacyl-, 44 ± 5 ms group of lipid chains; and choline compounds, 32 ± 9 ms.

Conclusion: An accurate knowledge of in vivo relaxation and J-coupling behavior will significantly improve the quantification of an extended number of resolved liver metabolites at 7 T.

Keywords: 7 T; J-coupling; STEAM; hepatic lipids; magnetic resonance spectroscopy; relaxation times.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adult
  • Body Water / chemistry*
  • Choline / analysis
  • Choline / chemistry*
  • Female
  • Humans
  • Lipids / analysis
  • Lipids / chemistry*
  • Liver / chemistry*
  • Magnetic Resonance Imaging / methods*
  • Male
  • Proton Magnetic Resonance Spectroscopy / methods*
  • Reference Values
  • Reproducibility of Results
  • Sensitivity and Specificity
  • Tissue Distribution

Substances

  • Lipids
  • Choline