Fatty acid ethyl esters induce intestinal epithelial barrier dysfunction via a reactive oxygen species-dependent mechanism in a three-dimensional cell culture model

PLoS One. 2013;8(3):e58561. doi: 10.1371/journal.pone.0058561. Epub 2013 Mar 19.

Abstract

Background & aims: Evidence is accumulating that ethanol and its oxidative metabolite, acetaldehyde, can disrupt intestinal epithelial integrity, an important factor contributing to ethanol-induced liver injury. However, ethanol can also be metabolized non-oxidatively generating phosphatidylethanol and fatty acid ethyl esters (FAEEs). This study aims to investigate the effects of FAEEs on barrier function, and to explore the role of oxidative stress as possible mechanism.

Methods: Epithelial permeability was assessed by paracellular flux of fluorescein isothiocyanate-conjugated dextran using live cell imaging. Cell integrity was evaluated by lactate dehydrogenase release. Localization and protein levels of ZO-1 and occludin were analyzed by immunofluorescence and cell-based ELISA, respectively. Intracellular oxidative stress and cellular ATP levels were measured by dichlorofluorescein and luciferase driven bioluminescence, respectively.

Results: In vitro, ethyl oleate and ethyl palmitate dose dependently increased permeability associated with disruption and decreased ZO-1 and occludin protein levels, respectively, and increased intracellular oxidative stress without compromising cell viability. These effects could partially be attenuated by pretreatment with the antioxidant, resveratrol, pointing to the role of oxidative stress in the FAEEs-induced intestinal barrier dysfunction.

Conclusions: These findings show that FAEEs can induce intestinal barrier dysfunction by disrupting the tight junctions, most likely via reactive oxygen species-dependent mechanism.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenosine Triphosphate / metabolism
  • Caco-2 Cells
  • Cell Culture Techniques
  • Cell Membrane Permeability / drug effects
  • Ethanol / metabolism
  • Ethanol / toxicity
  • Humans
  • Intestinal Mucosa / drug effects*
  • Intestinal Mucosa / physiopathology*
  • Models, Biological
  • Occludin / metabolism
  • Oleic Acids / metabolism
  • Oleic Acids / toxicity*
  • Oxidative Stress
  • Palmitic Acids / metabolism
  • Palmitic Acids / toxicity*
  • Reactive Oxygen Species / metabolism
  • Resveratrol
  • Stilbenes / pharmacology
  • Tight Junctions / drug effects
  • Tight Junctions / metabolism
  • Zonula Occludens-1 Protein / metabolism

Substances

  • OCLN protein, human
  • Occludin
  • Oleic Acids
  • Palmitic Acids
  • Reactive Oxygen Species
  • Stilbenes
  • TJP1 protein, human
  • Zonula Occludens-1 Protein
  • Ethanol
  • Adenosine Triphosphate
  • ethyl palmitate
  • Resveratrol
  • ethyl oleate

Grants and funding

This study was supported by Top Institute Food and Nutrition (http://www.tifn.nl), Wageningen, The Netherlands. The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.