Multiplex assay for condition-dependent changes in protein-protein interactions

Proc Natl Acad Sci U S A. 2012 Jun 5;109(23):9213-8. doi: 10.1073/pnas.1204952109. Epub 2012 May 21.

Abstract

Changes in protein-protein interactions that occur in response to environmental cues are difficult to uncover and have been poorly characterized to date. Here we describe a yeast-based assay that allows many binary protein interactions to be assessed in parallel and under various conditions. This method combines molecular bar-coding and tag array technology with the murine dihydrofolate reductase-based protein-fragment complementation assay. A total of 238 protein-fragment complementation assay strains, each representing a unique binary protein complex, were tagged with molecular barcodes, pooled, and then interrogated against a panel of 80 diverse small molecules. Our method successfully identified specific disruption of the Hom3:Fpr1 interaction by the immunosuppressant FK506, illustrating the assay's capacity to identify chemical inhibitors of protein-protein interactions. Among the additional findings was specific cellular depletion of the Dst1:Rbp9 complex by the anthracycline drug doxorubicin, but not by the related drug idarubicin. The assay also revealed chemical-induced accumulation of several binary multidrug transporter complexes that largely paralleled increases in transcript levels. Further assessment of two such interactions (Tpo1:Pdr5 and Snq2:Pdr5) in the presence of 1,246 unique chemical compounds revealed a positive correlation between drug lipophilicity and the drug response in yeast.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Computational Biology
  • DNA-Binding Proteins
  • Mice
  • Microarray Analysis
  • Protein Interaction Mapping / methods*
  • Protein Interaction Maps / genetics*
  • Real-Time Polymerase Chain Reaction
  • Receptors, Formyl Peptide / metabolism
  • Saccharomyces cerevisiae Proteins
  • Small Molecule Libraries / metabolism*
  • Tacrolimus
  • Tetrahydrofolate Dehydrogenase / metabolism*
  • Yeasts

Substances

  • DNA-Binding Proteins
  • DST1 protein, S cerevisiae
  • Fpr1 protein, mouse
  • Receptors, Formyl Peptide
  • Saccharomyces cerevisiae Proteins
  • Small Molecule Libraries
  • Tetrahydrofolate Dehydrogenase
  • Tacrolimus