A universal nucleoside with strong two-band switchable fluorescence and sensitivity to the environment for investigating DNA interactions

J Am Chem Soc. 2012 Jun 20;134(24):10209-13. doi: 10.1021/ja3030388. Epub 2012 Jun 4.

Abstract

With the aim of developing a new tool to investigate DNA interactions, a nucleoside analogue incorporating a 3-hydroxychromone (3HC) fluorophore as a nucleobase mimic was synthesized and incorporated into oligonucleotide chains. In comparison with existing fluorescent nucleoside analogues, this dye features exceptional environmental sensitivity switching between two well-resolved fluorescence bands. In labeled DNA, this nucleoside analogue does not alter the duplex conformation and exhibits a high fluorescence quantum yield. This probe is up to 50-fold brighter than 2-aminopurine, the fluorescent nucleoside standard. Moreover, the dual emission is highly sensitive to the polarity of the environment; thus, a strong shielding effect of the flanking bases from water was observed. With this nucleoside, the effect of a viral chaperone protein on DNA base stacking was site-selectively monitored.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Chromones / chemistry*
  • DNA / chemistry*
  • DNA / metabolism
  • Fluorescent Dyes / chemistry*
  • Nucleosides / chemistry*
  • Spectrometry, Fluorescence / methods

Substances

  • 3-hydroxychromone
  • Chromones
  • Fluorescent Dyes
  • Nucleosides
  • DNA