A simple, sensitive, rapid and specific detection method for Bisphenol A based on Fluorescence Polarization Immunoassay

Immunol Invest. 2012;41(1):38-50. doi: 10.3109/08820139.2011.579671. Epub 2011 May 26.

Abstract

A rapid, sensitive, specific and simple method based on Fluorescence Polarization Immunoassay (FPIA) was developed for the quantitative detection of Bisphenol A in water. 4, 4-Bis (4-hydroxyphenyl) valeric acid (BHPVA) was selected as the hapten to produce the immunogen. Fluorescein-labeled Bisphenol A derivatives (tracers) with different structures were synthesized and purified by thin layer chromatography. Based on the polyclonal antibody and tracers, an optimized FPIA method was developed with a detection limit (10% inhibition) of 2 μg L(-1) and a linear working range of 20 to 800 μg L(-1). FPIA was suitable for screening a large number of samples. The recoveries of fortified Tai lake water samples ranged from 91.85 to 102.78%, and tap water samples ranged from 90.36 to 96.01%. The coefficients of variation were all less than 20%. This FPIA method, which did not require a complicated cleanup process, proved to be very useful for the screening of Bisphenol A in environmental water samples.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Air Pollutants, Occupational / adverse effects
  • Air Pollutants, Occupational / analysis*
  • Benzhydryl Compounds
  • Drinking
  • Fluorescence Polarization Immunoassay*
  • High-Throughput Screening Assays
  • Humans
  • Lakes / chemistry
  • Occupational Medicine* / methods
  • Phenols / adverse effects
  • Phenols / analysis
  • Phenols / chemical synthesis*
  • Sensitivity and Specificity
  • Solutions / chemistry*

Substances

  • Air Pollutants, Occupational
  • Benzhydryl Compounds
  • Phenols
  • Solutions
  • bisphenol A