Purification, crystallization and data collection of Pectobacterium chrysanthemi AcsD, a type A siderophore synthetase

Acta Crystallogr Sect F Struct Biol Cryst Commun. 2008 Nov 1;64(Pt 11):1052-5. doi: 10.1107/S1744309108032132. Epub 2008 Oct 31.

Abstract

AcsD, a type A siderophore synthetase with a molecular weight of 71 140 Da from Pectobacterium chrysanthemi, has been expressed, purified and crystallized at 293 K. The protein crystallized in the primitive orthorhombic space group P2(1)2(1)2(1), with unit-cell parameters a = 80.3, b = 95.7, c = 161.1 A, alpha = beta = gamma = 90 degrees . Systematic absences were consistent with space group P2(1)2(1)2(1). A complete data set has been collected to 2.25 A resolution on BM14 at the ESRF. Consideration of the likely solvent content suggested that the asymmetric unit contained two molecules. Gel-filtration experiments indicated that the protein was a dimer, although self-rotation analyses did not detect a convincing twofold symmetry axis in the asymmetric unit. The protein has no convincing sequence match to any known structure and thus solution is likely to require experimental phasing.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / genetics
  • Crystallization
  • Dickeya chrysanthemi / enzymology*
  • Ligases / chemistry*
  • Ligases / genetics
  • Molecular Sequence Data
  • Molecular Structure
  • Siderophores / biosynthesis*
  • X-Ray Diffraction

Substances

  • Bacterial Proteins
  • Siderophores
  • Ligases