Effects of the JAK2 inhibitor, AZ960, on Pim/BAD/BCL-xL survival signaling in the human JAK2 V617F cell line SET-2

J Biol Chem. 2008 Nov 21;283(47):32334-43. doi: 10.1074/jbc.M803813200. Epub 2008 Sep 4.

Abstract

The Janus-associated kinase 2 (JAK2) V617F mutation is believed to play a critical role in the pathogenesis of polycythemia vera, essential thrombocythemia, and idiopathic myelofibrosis. We have characterized a novel small molecule JAK2 inhibitor, AZ960, and used it as a tool to investigate the consequences of JAK2 V617F inhibition in the SET-2 cell line. AZ960 inhibits JAK2 kinase with a K(i) of 0.00045 microm in vitro and treatment of TEL-JAK2 driven Ba/F3 cells with AZ960 blocked STAT5 phosphorylation and potently inhibited cell proliferation (GI(50)=0.025 microm). AZ960 demonstrated selectivity for TEL-JAK2-driven STAT5 phosphorylation and cell proliferation when compared with cell lines driven by similar fusions of the other JAK kinase family members. In the SET-2 human megakaryoblastic cell line, heterozygous for the JAK2 V617F allele, inhibition of JAK2 resulted in decreased STAT3/5 phosphorylation and inhibition of cell proliferation (GI(50)=0.033 microm) predominately through the induction of mitochondrial-mediated apoptosis. We provide evidence that JAK2 inhibition induces apoptosis by direct and indirect regulation of the anti-apoptotic protein BCL-xL. Inhibition of JAK2 blocked BCL-XL mRNA expression resulting in a reduction of BCL-xL protein levels. Additionally, inhibition of JAK2 resulted in decreased PIM1 and PIM2 mRNA expression. Decreased PIM1 mRNA corresponded with a decrease in Pim1 protein levels and inhibition of BAD phosphorylation at Ser(112). Finally, small interfering RNA-mediated suppression of BCL-xL resulted in apoptotic cell death similar to the phenotype observed following JAK2 inhibition. These results suggest a model in which JAK2 promotes cell survival by signaling through the Pim/BAD/BCL-xL pathway.

MeSH terms

  • Aminopyridines / pharmacology*
  • Apoptosis
  • Cell Line
  • Cell Line, Tumor
  • Cell Survival
  • Enzyme Inhibitors / pharmacology*
  • Gene Expression Regulation*
  • Humans
  • Janus Kinase 2 / antagonists & inhibitors*
  • Phenotype
  • Proto-Oncogene Proteins c-pim-1 / metabolism*
  • Pyrazoles / pharmacology*
  • RNA, Messenger / metabolism
  • RNA, Small Interfering / metabolism
  • Signal Transduction
  • bcl-Associated Death Protein / metabolism*
  • bcl-X Protein / metabolism*

Substances

  • 5-fluoro-2-(1-(4-fluorophenyl)ethylamino)-6-(5-methyl-1H-pyrazol-3-ylamino)nicotinonitrile
  • Aminopyridines
  • BAD protein, human
  • BCL2L1 protein, human
  • Enzyme Inhibitors
  • Pyrazoles
  • RNA, Messenger
  • RNA, Small Interfering
  • bcl-Associated Death Protein
  • bcl-X Protein
  • Janus Kinase 2
  • PIM1 protein, human
  • Proto-Oncogene Proteins c-pim-1