High-resolution crystal structure of an engineered human beta2-adrenergic G protein-coupled receptor

Science. 2007 Nov 23;318(5854):1258-65. doi: 10.1126/science.1150577. Epub 2007 Oct 25.

Abstract

Heterotrimeric guanine nucleotide-binding protein (G protein)-coupled receptors constitute the largest family of eukaryotic signal transduction proteins that communicate across the membrane. We report the crystal structure of a human beta2-adrenergic receptor-T4 lysozyme fusion protein bound to the partial inverse agonist carazolol at 2.4 angstrom resolution. The structure provides a high-resolution view of a human G protein-coupled receptor bound to a diffusible ligand. Ligand-binding site accessibility is enabled by the second extracellular loop, which is held out of the binding cavity by a pair of closely spaced disulfide bridges and a short helical segment within the loop. Cholesterol, a necessary component for crystallization, mediates an intriguing parallel association of receptor molecules in the crystal lattice. Although the location of carazolol in the beta2-adrenergic receptor is very similar to that of retinal in rhodopsin, structural differences in the ligand-binding site and other regions highlight the challenges in using rhodopsin as a template model for this large receptor family.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Bacteriophage T4 / enzymology
  • Binding Sites
  • Cell Membrane / chemistry
  • Cell Membrane / metabolism
  • Cholesterol / chemistry
  • Cholesterol / metabolism
  • Crystallization
  • Crystallography, X-Ray
  • Drug Inverse Agonism
  • Humans
  • Ligands
  • Models, Molecular
  • Muramidase / chemistry
  • Muramidase / metabolism
  • Propanolamines / chemistry
  • Propanolamines / metabolism
  • Protein Conformation
  • Protein Folding
  • Protein Structure, Secondary
  • Receptors, Adrenergic, beta-2 / chemistry*
  • Receptors, Adrenergic, beta-2 / metabolism
  • Recombinant Fusion Proteins / chemistry
  • Recombinant Fusion Proteins / metabolism
  • Rhodopsin / chemistry
  • Rhodopsin / metabolism
  • Static Electricity

Substances

  • Ligands
  • Propanolamines
  • Receptors, Adrenergic, beta-2
  • Recombinant Fusion Proteins
  • carazolol
  • Rhodopsin
  • Cholesterol
  • Muramidase

Associated data

  • PDB/2RH1