A kinetic method amenable to automation for ceruloplasmin estimation with inexpensive and stable reagents

Clin Biochem. 2007 May;40(8):571-4. doi: 10.1016/j.clinbiochem.2006.12.012. Epub 2007 Feb 8.

Abstract

Objectives: To develop a kinetic, inexpensive, automatable assay for ceruloplasmin as ferroxidase.

Design and methods: Dithiothreitol has been used to stabilize the substrate and quinolones to complex the ferric.

Results: Mean ferroxidase activity in healthy adults, Wilson's disease and pregnancy was 787.29, 178.5 and 1828.09 IU/L, respectively. Correlation coefficient of ferroxidase vis-à-vis copper, ferroxidase by ferrozine and ceruloplasmin were 0.90, 0.94 and 0.92, respectively.

Conclusions: Norfloxacin method is a simple, inexpensive and automatable kinetic assay.

MeSH terms

  • Adult
  • Ceruloplasmin / analysis*
  • Ceruloplasmin / metabolism*
  • Clinical Chemistry Tests / economics
  • Clinical Chemistry Tests / methods*
  • Dithiothreitol / chemistry
  • Female
  • Ferrozine / chemistry
  • Hepatolenticular Degeneration / enzymology
  • Humans
  • Hydrogen-Ion Concentration
  • Kinetics
  • Male
  • Norfloxacin / chemistry
  • Pregnancy
  • Quinolones / chemistry
  • Reproducibility of Results

Substances

  • Quinolones
  • Ferrozine
  • Ceruloplasmin
  • Norfloxacin
  • Dithiothreitol