High level expression of a recombinant phospholipase C from Bacillus cereus in Bacillus subtilis

Appl Microbiol Biotechnol. 2007 Mar;74(3):634-9. doi: 10.1007/s00253-006-0712-z. Epub 2006 Nov 18.

Abstract

Twenty-two Bacillus cereus strains were screened for phospholipase C (PLC, EC 3.1.4.3) activity using p-nitrophenyl phosphorylcholine as a substrate. Two strains (B. cereus SBUG 318 and SBUG 516) showed high activity at elevated temperatures (>70 degrees C) at acidic pH (pH 3.5-6) and were selected for cloning and functional expression using Bacillus subtilis. The genes were amplified from B. cereus DNA using primers based on a known PLC sequence and cloned into the expression vector pMSE3 followed by transformation into B. subtilis WB800. On the amino acid level, one protein (PLC318) was identical to a PLC described from B. cereus, whereas PLC516 contained an amino acid substitution (E173D). PLC production using the recombinant strains was performed by an acetoin-controlled expression system. For PLC516, 13.7 U g(-1) wet cell weight was determined in the culture supernatant after 30 h cultivation time. Three purification steps resulted in pure PLC516 with a specific activity of 13,190 U mg(-1) protein.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacillus cereus / enzymology*
  • Bacillus cereus / genetics
  • Bacillus subtilis / enzymology
  • Bacillus subtilis / genetics*
  • Cloning, Molecular
  • DNA, Bacterial / genetics
  • Enzyme Stability
  • Gene Expression
  • Genetic Vectors
  • Hot Temperature
  • Hydrogen-Ion Concentration
  • Phosphorylcholine / analogs & derivatives
  • Phosphorylcholine / metabolism
  • Polymerase Chain Reaction
  • Recombinant Proteins / biosynthesis
  • Sequence Homology, Amino Acid
  • Transformation, Bacterial
  • Type C Phospholipases / biosynthesis*
  • Type C Phospholipases / genetics
  • Type C Phospholipases / isolation & purification

Substances

  • 4-nitrophenylphosphorylcholine
  • DNA, Bacterial
  • Recombinant Proteins
  • Phosphorylcholine
  • Type C Phospholipases