Relative contribution of matrix metalloprotease and cysteine protease activities to cytokine-stimulated articular cartilage degradation

Osteoarthritis Cartilage. 2006 Aug;14(8):738-48. doi: 10.1016/j.joca.2006.01.016. Epub 2006 Mar 23.

Abstract

Objective: Both matrix metalloprotease (MMP) activity and cathepsin K (CK) activity have been implicated in cartilage turnover. We investigated the relative contribution of MMP activity and CK activity in cartilage degradation using ex vivo and in vivo models.

Methods: Bovine articular cartilage explants were stimulated with oncostatin M (OSM) 10 ng/ml and tumor necrosis factor-alpha (TNF-alpha) 20 ng/ml in the presence or absence of the broad-spectrum MMP inhibitor GM6001 and the cysteine protease inhibitor, E64. Cartilage degradation was evaluated in the conditioned medium by glycosaminoglycans (GAG), hydroxyproline, and cross-linked C-telopeptide fragments of type II collagen (CTX-II), which were compared to immunohistochemical evaluations of proteoglycans and CTX-II. We assessed MMP expression by gelatine zymography and CK expression by immunohistochemistry. In vivo, CTX-II release was measured from CK-deficient mice.

Results: OSM and TNF-alpha combined induced significant (P<0.01) increase in cartilage degradation products measured by hydroxyproline and CTX-II compared to vehicle control. The cytokines potently induced MMP expression, assessed by zymography, and CK expression investigated by immunohistochemistry. Inhibition of MMP activity completely abrogated hydroxyproline and CTX-II release (P<0.01) and GAG release (P<0.05). In contrast, E64 resulted in increased CTX-II release by 100% (P<0.05) and inhibited GAG release by 30%. Up-regulation of CTX-II fragments was confirmed in vivo in CK null mice.

Conclusion: Inhibition of MMP activity reduced both proteoglycan loss and type II collagen degradation. In contrast, inhibition of cysteine proteases resulted in an increase rather than a decrease in MMP derived fragments of collagen type II degradation, CTX-II, suggesting altered collagen metabolism.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Arthritis, Experimental
  • Biomarkers / analysis
  • Cartilage, Articular / drug effects
  • Cartilage, Articular / enzymology*
  • Cathepsin K
  • Cathepsins / deficiency
  • Cathepsins / metabolism
  • Cattle
  • Collagen Type I / analysis
  • Cysteine Endopeptidases / metabolism*
  • Cysteine Proteinase Inhibitors / pharmacology
  • Cytokines / pharmacology*
  • Dipeptides / pharmacology
  • Extracellular Matrix / enzymology
  • Extracellular Matrix / immunology*
  • Glycosaminoglycans / analysis
  • Hydroxyproline / analysis
  • Immunohistochemistry / methods
  • Leucine / analogs & derivatives
  • Leucine / pharmacology
  • Matrix Metalloproteinase Inhibitors
  • Matrix Metalloproteinases / metabolism*
  • Mice
  • Mice, Knockout
  • Oncostatin M / pharmacology
  • Osteoarthritis, Knee / enzymology
  • Osteoarthritis, Knee / immunology*
  • Peptides / analysis
  • Stimulation, Chemical
  • Tissue Culture Techniques
  • Tumor Necrosis Factor-alpha / pharmacology

Substances

  • Biomarkers
  • Collagen Type I
  • Cysteine Proteinase Inhibitors
  • Cytokines
  • Dipeptides
  • Glycosaminoglycans
  • Matrix Metalloproteinase Inhibitors
  • N-(2(R)-2-(hydroxamidocarbonylmethyl)-4-methylpentanoyl)-L-tryptophan methylamide
  • Peptides
  • Tumor Necrosis Factor-alpha
  • collagen type I trimeric cross-linked peptide
  • Oncostatin M
  • N-(N-(3-carboxyoxirane-2-carbonyl)leucyl)isoamylamine
  • Cathepsins
  • Cysteine Endopeptidases
  • Cathepsin K
  • Ctsk protein, mouse
  • Matrix Metalloproteinases
  • Leucine
  • Hydroxyproline