Structural basis of affinity maturation and intramolecular cooperativity in a protein-protein interaction

Structure. 2005 Dec;13(12):1775-87. doi: 10.1016/j.str.2005.08.015.

Abstract

Although protein-protein interactions are involved in nearly all cellular processes, general rules for describing affinity and selectivity in protein-protein complexes are lacking, primarily because correlations between changes in protein structure and binding energetics have not been well determined. Here, we establish the structural basis of affinity maturation for a protein-protein interaction system that we had previously characterized energetically. This model system exhibits a 1500-fold affinity increase. Also, its affinity maturation is restricted by negative intramolecular cooperativity. With three complex and six unliganded variant X-ray crystal structures, we provide molecular snapshots of protein interface remodeling events that span the breadth of the affinity maturation process and present a comprehensive structural view of affinity maturation. Correlating crystallographically observed structural changes with measured energetic changes reveals molecular bases for affinity maturation, intramolecular cooperativity, and context-dependent binding.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Substitution
  • Animals
  • Crystallography, X-Ray
  • Enterotoxins / chemistry*
  • Enterotoxins / genetics
  • Mice
  • Models, Molecular*
  • Mutation
  • Peptide Fragments / chemistry*
  • Peptide Fragments / genetics
  • Protein Conformation
  • Protein Interaction Mapping*
  • Receptors, Antigen, T-Cell, alpha-beta / chemistry*
  • Receptors, Antigen, T-Cell, alpha-beta / genetics
  • Water / chemistry

Substances

  • Enterotoxins
  • Peptide Fragments
  • Receptors, Antigen, T-Cell, alpha-beta
  • T-cell receptor Vbeta 8.2
  • Water
  • enterotoxin C, staphylococcal

Associated data

  • PDB/2APB
  • PDB/2APF
  • PDB/2APT
  • PDB/2APV
  • PDB/2APW
  • PDB/2APX
  • PDB/2AQ1
  • PDB/2AQ2
  • PDB/2AQ3