Purification and characterization of a low-Km 3':5'-cyclic adenosine phosphodiesterase from post-meiotic male mouse germ cells

Biochim Biophys Acta. 1992 May 22;1121(1-2):178-82. doi: 10.1016/0167-4838(92)90352-e.

Abstract

We describe the purification and the study of the kinetic and hydrodynamic properties of a 'low Km' cAMP phosphodiesterase specifically expressed in haploid male germ cells of the mouse. The enzyme has been purified approx. 13,000-fold with respect to the activity in total cell homogenate. The purified enzyme hydrolyzed specifically cAMP with a Km of 3.3 microM and with a Vmax of 10.5 mumol of cAMP hydrolyzed/min per mg of protein. The hydrolytic activity was neither stimulated nor inhibited by cGMP, whereas it was inhibited by RO 20-1724 and Rolipram. The enzyme showed a Stokes radius of 3.8 nm and a sedimentation coefficient of 3.1 S, corresponding to a native molecular mass of 50 kDa and a frictional ratio of 1.53. Sodium dodecyl sulphate polyacrylamide gel electrophoresis analysis of sucrose gradient fractions of the purified enzyme showed a major band of 43 kDa copeaking with enzyme activity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • 3',5'-Cyclic-AMP Phosphodiesterases / isolation & purification*
  • 3',5'-Cyclic-AMP Phosphodiesterases / metabolism*
  • 4-(3-Butoxy-4-methoxybenzyl)-2-imidazolidinone / pharmacology
  • Animals
  • Centrifugation, Density Gradient
  • Chromatography, Affinity
  • Chromatography, DEAE-Cellulose
  • Chromatography, Gel
  • Cytosol / enzymology
  • Kinetics
  • Male
  • Mice
  • Mice, Inbred Strains
  • Molecular Weight
  • Phosphodiesterase Inhibitors / pharmacology
  • Protein Conformation
  • Pyrrolidinones / pharmacology
  • Rolipram
  • Testis / enzymology*

Substances

  • Phosphodiesterase Inhibitors
  • Pyrrolidinones
  • 4-(3-Butoxy-4-methoxybenzyl)-2-imidazolidinone
  • 3',5'-Cyclic-AMP Phosphodiesterases
  • Rolipram