A novel potassium sensing in aqueous media with a synthetic oligonucleotide derivative. Fluorescence resonance energy transfer associated with Guanine quartet-potassium ion complex formation

J Am Chem Soc. 2002 Dec 4;124(48):14286-7. doi: 10.1021/ja026892f.

Abstract

A novel potassium sensing oligonucleotide (PSO) was constructed by attaching fluorophores 6-FAM and 6-TAMRA to the 5'- and 3'-termini of d(GGG TTA GGG TTA GGG TTA GGG), respectively. The affinity of PSO for K+ was 43 000 times greater than that for Na+, high enough selectivity enabling quantitation of K+ specifically in the presence of excess Na+. Fluorescence resonance energy transfer (FRET) to 6-TAMRA from 6-FAM of PSO was observed only in the presence of K+. This phenomenon is based on the approximation of the two fluorophores upon formation of a guanine quartet mediated by K+. Furthermore, the fluorescent color of PSO changes from yellow to red upon formation of the complex, thereby enabling visualization of K+ in aqueous media.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Binding Sites
  • Energy Transfer
  • Fluoresceins / chemistry
  • Fluorescent Dyes / chemistry*
  • Guanine / chemistry*
  • Guanine / metabolism
  • Humans
  • Kinetics
  • Oligonucleotides / chemistry*
  • Oligonucleotides / metabolism
  • Potassium / analysis*
  • Potassium / chemistry
  • Potassium / metabolism
  • Rhodamines / chemistry
  • Spectrometry, Fluorescence / methods
  • Telomere / genetics
  • Water / chemistry

Substances

  • 6-carboxytetramethylrhodamine
  • Fluoresceins
  • Fluorescent Dyes
  • Oligonucleotides
  • Rhodamines
  • Water
  • 6-carboxyfluorescein
  • Guanine
  • Potassium