Multifrequency probe for pulsed EPR and ENDOR spectroscopy

J Magn Reson. 2001 Dec;153(2):178-85. doi: 10.1006/jmre.2001.2450.

Abstract

The design, construction, and performance of a multifrequency pulsed EPR and ENDOR probe for use at cryogenic temperatures are described. Interchangeable resonators based on a folded strip line design allow variation of the resonance frequency over a range of 5-11 GHz. Variable coupling to the resonator is achieved capacitively via a simple mechanical adjustment which is thermally and mechanically stable. The entire assembly is robust and easily fabricated. Common methods of analyzing the resonator parameters such as the Q-factor and coupling coefficient are discussed quantitatively. Probe performance data and multifrequency pulsed ENDOR spectra are presented.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Electron Spin Resonance Spectroscopy / instrumentation*
  • Equipment Design
  • Temperature