The purification, crystallization and preliminary structural characterization of glucose-1-phosphate thymidylyltransferase (RmlA), the first enzyme of the dTDP-L-rhamnose synthesis pathway from Pseudomonas aeruginosa

Acta Crystallogr D Biol Crystallogr. 2000 Nov;56(Pt 11):1501-4. doi: 10.1107/s0907444900010040.

Abstract

Glucose-1-phosphate thymidylyltransferase (RmlA; E.C. 2.7.7.24) is the first of four enzymes involved in the biosynthesis of dTDP-L-rhamnose, the precursor of L-rhamnose, a key component of the cell wall of many pathogenic bacteria. RmlA catalyses the condensation of thymidine triphosphate (dTTP) and alpha-D-glucose-1-phosphate (G1P), yielding dTDP-D-glucose. RmlA from Pseudomonas aeruginosa has been overexpressed and purified. Crystals of the enzyme have been grown using the sitting-drop vapour-diffusion technique with PEG 6000 and lithium sulfate as precipitant. Several diffraction data sets of single frozen crystals were collected to a resolution of 1.66 A. Crystals belonged to space group P1, with unit-cell parameters a = 71.5, b = 73.1, c = 134.7 A, alpha = 89.9, beta = 80.9, gamma = 81.1 degrees. The asymmetric unit contains eight monomers in the form of two RmlA tetramers with a solvent content of 51%. Selenomethionine-labelled protein has been obtained and crystallized.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Chromatography, High Pressure Liquid
  • Crystallization
  • Crystallography, X-Ray
  • Nucleoside Diphosphate Sugars / biosynthesis*
  • Nucleotidyltransferases / chemistry
  • Nucleotidyltransferases / isolation & purification*
  • Protein Conformation
  • Pseudomonas aeruginosa / enzymology*
  • Thymine Nucleotides / biosynthesis*

Substances

  • Nucleoside Diphosphate Sugars
  • Thymine Nucleotides
  • thymidine diphosphate rhamnose
  • Nucleotidyltransferases
  • glucose-1-phosphate thymidylyltransferase